HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glyoxal → HCID 15099952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glyoxal | HCID 7860 | — |
| Reactant | HCID 19877669 | HCID 19877669 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15099952 | HCID 15099952 | 90% |
Reaction Steps
Following the procedure of Example 2, mononeohexyl phosphine (200 parts) in tetrahydrofuran, is reacted with 250 parts of glyoxal and 256 parts (90% yield) of 1,4-di-N-eohexyl-2,3,5,6-tetrahydroxy-1,4-diphosphorinane, m.p. 186°-210° C., are isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05149878 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-dc4dce65f7884e589844eb1252c53c60 |
| Source note | uspto-grants-1992_09 |