Glyoxal → HCID 15099955, compound

HRID 1886235Notes

Reaction equation

[CH2:1]([PH2:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH:10]([CH:12]=[O:13])=[O:11]>>[CH2:1]([P:9]1[CH:10]([OH:11])[CH:12]([OH:13])[P:9]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH:10]([OH:11])[CH:12]1[OH:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

Reactant 2

HCID 7860Glyoxal

HCID 446269Phosphine, octyl-

Product 1

HCID 15099955HCID 15099955, compound

Procedure

Following the procedure of Example 1, 200 parts of mono-n-octylphosphine is reacted with 194 parts of glyoxal to give 1,4-di-n-octyl-2,3,5,6-tetrahydroxy-1,4-diphosphorinane, a waxy solid.

Sources & evidence

ORD record: ord-f9bd221ed4e8405f91a2b0f058b25984
Source dataset: uspto-grants-1992_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05149878

Reaction notes

Loading…