N-Methylbutylamine → 6-Bromo-N-butyl-N-methylhexanamide

HRID 1886246Notes

Reaction equation

[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=O.[CH3:10][NH:11][CH2:12][CH2:13][CH2:14][CH3:15]>>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([N:11]([CH2:12][CH2:13][CH2:14][CH3:15])[CH3:10])=[O:9]

Participants

Reactant 2

HCID 8068N-Methylbutylamine

HCID 202106-Bromohexanoic acid

Product 1

HCID 226727536-Bromo-N-butyl-N-methylhexanamide

Procedure

Using the procedure of Step A of Example 3, 4.88 g of 6-bromohexanoic acid and 4.36 ml of N-methylbutylamine were reacted to obtain 7.0 g of the expected product which was used as is for the following step.

Workup

customwere reacted

Sources & evidence

ORD record: ord-79ad2dcc1564421a89fa85b4556bcba2
Source dataset: uspto-grants-1992_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05149696

Reaction notes

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