HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Cyanobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Cyanobenzoic acid | HCID 138061 | — |
| Product | 2-Cyanobenzoyl chloride | HCID 119681 | — |
Reaction Steps
A mixture of 2-cyanobenzoic acid (2 g, 13.6 mmol) and 15 ml of thionyl chloride was refluxed overnight. Excess thionyl chloride was removed in vacuo and the resultant 2-cyanobenzoyl chloride obtained as such as an off white solid was used in the above acylation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05151435 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-d10a601e621143c5878456b0a3418d7b |
| Source note | uspto-grants-1992_09 |