HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 57626096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Methoxy-4-(2-(pyrrolidin-1-yl)ethoxy)aniline | HCID 11736503 | — |
| Reactant | 6-[(S)-1-(Tetrahydrofuran-2-yl)methoxy]isochroman-1-one | HCID 66679924 | — |
| Product | HCID 57626096 | HCID 57626096 | — |
Reaction Steps
6-[(S)-1-(Tetrahydrofuran-2-yl)methoxy]isochroman-1-one was firstly converted with thionyl chloride by method B into the corresponding dichloride, and then reacted with 3-methoxy-4-(2-pyrrolidin-1-ylethoxy)phenylamine by method A. The product with the molecular weight of 466.58 (C27H34N2O5) was obtained in this way; MS (ESI): 467 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501771B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-777b3103fcc04b63880b709dc679f6b6 |
| Source note | uspto-grants-2013_08 |