HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Difluorobenzoyl chloride → HCID 71208641, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Difluorobenzoyl chloride | HCID 588082 | — |
| Reactant | 3-(aminomethyl)-7-chloro-1-phenylquinolin-4(1H)-one | HCID 71208398 | — |
| Product | HCID 71208641 | HCID 71208641 | — |
Reaction Steps
N-(7-Chloro-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)-2,5-difluoro-benzamide was prepared starting from intermediate D and 2,5-difluoro-benzoyl chloride. 1H NMR (400 MHz, DMSO-d6) δ ppm 8.70 (br. s., 1H) 8.28 (d, J=8.66 Hz, 1H) 8.00 (s, 1H) 7.53-7.79 (m, 5 H) 7.21-7.52 (m, 4H) 6.92 (d, J=1.81 Hz, 1H) 4.39 (d, J=5.64 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501732B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-6807af82f885459896574f0a499d9dcf |
| Source note | uspto-grants-2013_08 |