Acetyl chloride → HCID 178473789, compound

Participants

Reaction Steps

This compound was prepared in a fashion analogous to the procedure described in Example 4. Thus, 5-phenyl-3-(4-piperidinyl)-1H-indazole-7-carboxamide hydrochloride (0.057 g, 0.17 mmol) was reacted with acetyl chloride (0.012 mL, 0.17 mmol) in the presence of triethylamine (0.1 mL, 0.71 mmol) and DMAP (0.0021 g, 0.017 mmol) in DMF (3 mL) to give 0.030 g of a white solid.

Provenance & Evidence