HCID 20975526, compound → HCID 68771976, compound

HRID 1888315Notes

Reaction equation

HRID 1888315 reaction equation
[OH:1][C@H:2]1[CH2:6][CH2:5][C@H:4](/[CH:7]=[CH:8]/[CH2:9][C:10]([CH3:23])([O:16][CH:17]2[CH2:22][CH2:21][CH2:20][CH2:19][O:18]2)[CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C@H:3]1[CH2:24][CH2:25][S:26][C:27]1[S:28][CH:29]=[C:30]([C:32]([OH:34])=[O:33])[N:31]=1.[I-].[CH4:36]>>[OH:1][C@H:2]1[CH2:6][CH2:5][C@H:4](/[CH:7]=[CH:8]/[CH2:9][C:10]([CH3:23])([O:16][CH:17]2[CH2:22][CH2:21][CH2:20][CH2:19][O:18]2)[CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C@H:3]1[CH2:24][CH2:25][S:26][C:27]1[S:28][CH:29]=[C:30]([C:32]([O:34][CH3:36])=[O:33])[N:31]=1

Participants

3

Reactant 2

HCID 20975526HCID 20975526, compoundHCID 66858527HCID 66858527, compound

Product 1

HCID 68771976HCID 68771976, compound

Procedure

By the same procedure as the reaction of Example 51 using the compound 55 instead of the compound 50 and using methane iodide instead of ethane iodide, the title compound having the following physical data was obtained.

Sources & evidence

ORD record
ord-81e7023aafd848d5925ebce53122bd37
Source dataset
uspto-grants-2013_08
Patent number
US08501793B2

Reaction notes

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