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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 18884Generated: October 30, 2026

4-Methoxybenzenesulfonyl chloride → HCID 11212994, compound

https://huagongshe.com/reaction/18884

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Methoxybenzenesulfonyl chlorideHCID 7401—
Reactant(2-Amino-4-bromophenyl)(phenyl)methanoneHCID 4149946—
ProductHCID 11212994HCID 11212994—

Reaction Steps

The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 138 mg of (2-Amino-4-bromo-phenyl)-phenyl-methanone and 103 mg of 4-Methoxy-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 3.72 (s, 3H), 6.75 (d, 2H, J=8.8 Hz), 7.19-7,26 (m, 2H), 7.37-7.43 (m, 4H), 7.57 (m, 1H), 7.65 (d, 2H, J=8.8 Hz), 7.96 (s, 1H), 10.09 (s, 1H). MS: m/z 447.9 (M++1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07741519B2
Source datasetuspto-grants-2010_06
ORD IDord-724b153203ef48d5b32d1662d478db08
Source noteuspto-grants-2010_06