HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 3-[(1-Methylcyclopropyl)methyl]-5,6,7,8-tetrahydro-5,8-ethanocinnoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Bicyclo[2.2.2]octane-2,3-dione | HCID 548936 | — |
| Reactant | [3-(1-Methyl-cyclopropyl)-2-oxo-propyl]-phosphonic acid dim ethyl ester | HCID 86638118 | — |
| Product | 3-[(1-Methylcyclopropyl)methyl]-5,6,7,8-tetrahydro-5,8-ethanocinnoline | HCID 46175329 | — |
Reaction Steps
Light-yellow solid MS (ESI): 229.2 (MH+). Prepared from bicyclo[2.2.2]octane-2,3-dione, [3-(1-methyl-cyclopropyl)-2-oxo-propyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501940B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-6c9e30eabc61499f932ce55a0fac74b5 |
| Source note | uspto-grants-2013_08 |