HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58014784, compound → HCID 58014932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58014784 | HCID 58014784 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 58014932 | HCID 58014932 | 104.7% |
Reaction Steps
A solution of tert-butyl 4-((2-(4-(4-acetylpiperazin-1-yl)phenylamino)-5-carbamoylpyrimidin-4-ylamino)methyl)piperidine-1-carboxylate (0.105 g, 0.190 mmol) in TFA (2 mL) was stirred at room temperature for 4 h. TFA was removed in vacuo. The residue was purified by HPLC to give the titled compound (90 mg). MS 453.41 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501944B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-77d0c5e97f8f42d8b081587621671800 |
| Source note | uspto-grants-2013_08 |