HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58014932, compound → HCID 58014891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58014932 | HCID 58014932 | — |
| Reactant | HCID 178418250 | HCID 178418250 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 58014891 | HCID 58014891 | 29.4% |
Reaction Steps
A mixture of 2-(4-(4-acetylpiperazin-1-yl)phenylamino)-4-(piperidin-4-ylmethylamino)pyrimidine-5-carboxamide (25 mg, 0.055 mmol) and KOCN (20 mg, 0.25 mmol) in acetic acid (2 mL) was stirred at 100 C for 4 h. The mixture was then purified by HPLC to give the titled compound (8 mg). MS 496.45 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501944B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-5ccf685bc3a24931b7ae935e8b7c58fc |
| Source note | uspto-grants-2013_08 |