HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4,5-Trimethoxybenzaldehyde → HCID 178492117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4,5-Trimethoxybenzaldehyde | HCID 6858 | — |
| Reactant | N-(2-amino-5-(pyrrolidin-1-yl)phenyl)benzamide | HCID 68515788 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178492117 | HCID 178492117 | — |
Reaction Steps
A mixture of N-(2-amino-5-(pyrrolidin-1-yl)phenyl)benzamide (2 mmol) and 3,4,5-trimethoxybenzaldehyde (3 mmol) in methanol was stirred at room temperature for 12 h. The suspension was filtered and the solid was washed with methanol to afford (E)-N-(5-(pyrrolidin-1-yl)-2-(3,4,5-trimethoxybenzylideneamino)phenyl)benzamide as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501957B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-f9f3e722f3574204b664c4ca1e296603 |
| Source note | uspto-grants-2013_08 |