HRID1888967

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID180

Acetone

C3H6O

反应SMILES：N#C[C@@H]1C[C@@H]2C[C@@H]2N1C(=O)[C@@H](N)C12CC3CC(CC(O)(C3)C1)C2

HCID11243969

Saxagliptin

C18H25N3O2

PRODUCTS

产物

反应SMILES：CC(C)=N[C@H](C(=O)N1[C@H](C#N)C[C@@H]2C[C@@H]21)C12CC3CC(CC(O)(C3)C1)C2

HCID54577999

未命名化合物

PROCEDURE

实验过程

Saxagliptine form H-1 (100 mg) was suspended in acetone (1 ml). The suspension was stirred for 24 hours at room temperature, after which it was filtered and dried on air, yielding 54 mg of crystalline product

WORKUP

后处理

filtrationafter which it was filtered
customdried on air