HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tricyclohexylphosphine → HCID 86644014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tricyclohexylphosphine | HCID 75806 | — |
| Reactant | HCID 86608892 | HCID 86608892 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86644014 | HCID 86644014 | 64.4% |
Reaction Steps
To 25 ml of a solution of 12 mmol tricyclohexyl phosphine prepared in diethylether (as in example 2) is added 1.4 g (12 mmol) trifluoride acetic acid. After some time, a crystalline solid is precipitated, which is filtered off, and washed with a little diethylether. 2.4 g (59%) of a colorless solid is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501985B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-83c7943f761e4ffc89a2a804d6ae41b2 |
| Source note | uspto-grants-2013_08 |