HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 68478277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Tricyclohexylphosphine | HCID 75806 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 68478277 | HCID 68478277 | — |
Reaction Steps
1.2 g (12 mmol) concentrated sulfuric acid are added to 25 ml of a solution of 12 mmol tricyclohexyl phosphine in diethylether prepared as in comparative example 3. The initially formed smudgy mass crystallizes over time, and can then be filtered off. 4.5 g of a colorless hygroscopic solid is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501985B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-9479b0dfc5d94dd8bec63a006a56de68 |
| Source note | uspto-grants-2013_08 |