HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1890218Generated: October 30, 2026
Phosphorus sulfide (P2S5) → HCID 58422720, compound
https://huagongshe.com/reaction/1890218
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| Reactant | 2-Propyl-1-heptanol | HCID 24847 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 58422720 | HCID 58422720 | — |
Reaction Steps
0.2 mol of diphosphorus pentasulfide (44 g) was suspended in 300 ml of toluene and heated to 75° C. Then 0.8 mol of 2-propylheptanol (127 g) was added dropwise with evolution of gas over a period of 1 h. The reaction mixture was stirred at 75° C. for a further 2 hours. A clear solution was obtained. The conversion was >95% (determined by means of acid-base titration).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08507419B2 |
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| Source dataset | uspto-grants-2013_08 |
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| ORD ID | ord-d1337c852c2441fc99c40b25ebcdcd7e |
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| Source note | uspto-grants-2013_08 |
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