HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2,6-Diethyl-4-methylbenzyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2,6-Diethyl-4-methylbenzyl alcohol | HCID 66707540 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2,6-Diethyl-4-methylbenzyl chloride | HCID 66707697 | 158.3% |
Reaction Steps
To a mixture of 138.41 g of 2,6-diethyl-4-methylbenzyl alcohol and 820 g of toluene was added dropwise 60.96 g of thionyl chloride at 25° C. over 4.5 hours. The resultant mixture was stirred for 15 hours. The reaction mixture was concentrated to obtain 159.58 g of 2,6-diethyl-4-methylbenzyl chloride (GC-area: 71%) as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507410B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-8a9772cead8647128b59ef23caf641f5 |
| Source note | uspto-grants-2013_08 |