HCID 178526705, compound → HCID 178507772, compound

Participants

Reaction Steps

5-Nitro-6-(2-(trifluoromethoxy)phenylamino)pyridin-2-ol (400 mg, 1.27 mmol) and methanol (370 mL) were stirred at 25° C. for 4 h with excess Raney nickel under an atmosphere of hydrogen. After 4 h the solution was filtered by vacuum filtration through celite. The filtrate was concentrated under reduced pressure to give the title compound as a dark green solid (300 mg). LCMS m/z=286.2 [M+H]+.

Provenance & Evidence