Hydrochloric Acid → HCID 178515766, compound

Participants

Reaction Steps

5-(Benzyloxy)-3-(2,2-difluorocycloheptyl)-3H-imidazo[4,5-b]pyridine was dissolved in DCM and diluted with excess sulfuric acid. The resulting solution was stirred overnight at room temperature then acidified with the addition of 1 M aqueous hydrochloric acid. The solvent was removed from the organic layer and the residue was purified via preparative HPLC to give the title compound. LCMS m/z=267.9 [M+H]+.

Provenance & Evidence