HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1890512Generated: November 2, 2026
Ammonia methanol → Thieno[3,2-b]pyridin-2-ylmethanamine
https://huagongshe.com/reaction/1890512
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia methanol | HCID 21705897 | — |
| Reactant | HCID 67305098 | HCID 67305098 | — |
| Product | Thieno[3,2-b]pyridin-2-ylmethanamine | HCID 67305714 | — |
Reaction Steps
2-(Chloromethyl)thieno[3,2-b]pyridine (C-5) (183 mg, 1 mmol) was dissolved in NH3/methanol (7 N, 10 mL). The resulting mixture was stirred at 50° C. for 16 hours and concentrated. The residue was purified by chromatography. MS (m/z): 165 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08507487B2 |
|---|
| Source dataset | uspto-grants-2013_08 |
|---|
| ORD ID | ord-616b855999234ff7bc22f07f128c1c85 |
|---|
| Source note | uspto-grants-2013_08 |
|---|
