HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Ethyl 2-(2,4-difluorophenyl)acetimidate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2,4-Difluorophenylacetonitrile | HCID 69565 | — |
| Product | Ethyl 2-(2,4-difluorophenyl)acetimidate hydrochloride | HCID 67548940 | — |
Reaction Steps
Commercially available 2-(2,4-difluorophenyl)acetonitrile (Aldrich), HCl gas and ethanol were processed using the method described for Example 3A to obtain the titled compound except that the reaction time was 72 hours. MS (ESI+) m/z 200 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507493B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-5d0e595c88d541f780793188d692f7b7 |
| Source note | uspto-grants-2013_08 |