HRID1891079

反应详情

EQUATION

反应方程式

HRID 1891079 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

1.5 g (6.5 mmol) of (RS)—S-(2-methoxy-4-nitrophenyl)-S-methylsulfoximide in 100 ml of ethanol is mixed with 300 mg of palladium on carbon (10%×50% H2O) and hydrogenated for 45 minutes at room temperature and normal pressure. The batch is filtered and concentrated by evaporation. 1.0 g (5.1 mmol, corresponding to 79% of theory) of the product is obtained.

WORKUP

后处理

  1. filtrationThe batch is filtered
  2. concentrationconcentrated by evaporation
  3. custom1.0 g (5.1 mmol, corresponding to 79% of theory) of the product is obtained