HRID1891079
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
1.5 g (6.5 mmol) of (RS)—S-(2-methoxy-4-nitrophenyl)-S-methylsulfoximide in 100 ml of ethanol is mixed with 300 mg of palladium on carbon (10%×50% H2O) and hydrogenated for 45 minutes at room temperature and normal pressure. The batch is filtered and concentrated by evaporation. 1.0 g (5.1 mmol, corresponding to 79% of theory) of the product is obtained.
WORKUP
后处理
- filtrationThe batch is filtered
- concentrationconcentrated by evaporation
- custom1.0 g (5.1 mmol, corresponding to 79% of theory) of the product is obtained