Potassium Hydroxide → HCID 44612466, compound

HRID 1891999Notes

Reaction equation

[OH-].[K+].[Cl:3][C:4]1[CH:5]=[C:6]([C:11]2([CH3:23])[C:16]([C:17]([O:19]C)=[O:18])=[C:15]([CH3:21])[CH2:14][CH:13]([CH3:22])[CH2:12]2)[CH:7]=[CH:8][C:9]=1[Cl:10]>>[Cl:3][C:4]1[CH:5]=[C:6]([C:11]2([CH3:23])[C:16]([C:17]([OH:19])=[O:18])=[C:15]([CH3:21])[CH2:14][CH:13]([CH3:22])[CH2:12]2)[CH:7]=[CH:8][C:9]=1[Cl:10]

Participants

Reactant 2

HCID 14797Potassium Hydroxide

HCID 86653595HCID 86653595, compound

Product 1

HCID 44612466HCID 44612466, compound

Procedure

Following the procedure of Step 7, Example 1-3, (except that potassium hydroxide was used in place of sodium hydroxide), methyl (4RS,6RS)-6-(3,4-dichlorophenyl)-2,4,6-trimethylcyclohex-1-enecarboxylate was converted to Example 6. Mass spectrum m/z 313.14 (M+H+).

Sources & evidence

ORD record: ord-6da4e96c94be44689134e2c66ddf5ac3
Source dataset: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08507559B2

Reaction notes

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