Acetic Anhydride → HCID 178516711, compound
Reaction equation
[N:1]([N:3]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH2:4][C:5]([OH:7])=[O:6])=O.C(OC(=O)C)(=O)C>>[C:8]1([N+:3]2[N-:1][O:6][C:5](=[O:7])[CH:4]=2)[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1Participants
3
Procedure
N-phenyl sydnone was prepared by dehydration of the above prepared N-nitrosophenylglycine with acetic anhydride, using the method described in Organic Syntheses, Coll. Vol. 5, p. 962 (1973); Vol. 45, p. 96 (1965).
Sources & evidence
- ORD record
- ord-ac8910bbb0e048d0b5bb7069567120ce
- Source dataset
- uspto-grants-2013_08
- Patent number
- US08507570B2
Reaction notes
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