HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 1547824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 1H,3H-Naphtho(1,8-cd)pyran-1,3-dione, 6-bromo- | HCID 66493 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 1547824 | HCID 1547824 | — |
Reaction Steps
A mixture of 4-bromo-1,8-naphthalic anhydride (10 g), aniline (3.54 g) and acetic acid (75 ml) was refluxed with stirring for 10 hrs. The reaction mixture was then cooled to room temperature, whereupon solid separated out. The solid was filtered, washed with water (50 ml) followed by acetic acid (50 ml) and dried at 100° C. for 8 hours (Yield=10.8 gm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507590B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-eacbfc967e6a4217bf49d4a55bca4f5c |
| Source note | uspto-grants-2013_08 |