HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 2-Hydrazinyl-4-isopropyl-5,8-dimethylquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 2-Chloro-4-isopropyl-5,8-dimethylquinoline | HCID 83527054 | — |
| Product | 2-Hydrazinyl-4-isopropyl-5,8-dimethylquinoline | HCID 67083099 | — |
Reaction Steps
A solution of 2-chloro-4-isopropyl-5,8-dimethylquinoline (1.00 g, 4.3 mmol) in NH2NH2 was reacted as outlined in Scheme 1 above to give the title compound. Spectroscopic data: 1H NMR (300 MHz, CDCl3) δ ppm 1.30 (d, J=6.74 Hz, 6 H) 2.64 (s, 3 H) 2.82 (s, 3 H) 3.95-4.10 (m, 1 H) 6.72 (s, 1 H) 6.98 (d, J=7.33 Hz, 1 H) 7.30 (d, J=7.33 Hz, 1 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507682B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-0551ff0ccc79467eb062e1e71c340e20 |
| Source note | uspto-grants-2013_08 |