HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fipronil → Fipronil sulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fipronil | HCID 3352 | — |
| Reactant | 4-Amino-3,5-dichlorobenzotrifluoride | HCID 141094 | — |
| Product | Fipronil sulfide | HCID 9953940 | — |
Reaction Steps
European Patent publication No. 295117 describes the preparation of 5-amino-1-(2,6-dichloro-4-trifluoromethylphenyl)-3-cyano-4-trifluoromethylsulphinyl pyrazole starting from 2,6-Dichloro-4-trifluoromethylaniline to give an intermediate 5-amino-1-(2,6-dichloro-4-trifluoromethylphenyl)-3-cyano-4-trifluoromethylthiopyrazole which is oxidized with meta-chloroperbenzoic acid in chloroform to give desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507693B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-cb682b6fc7044de8987863b017c9b8f0 |
| Source note | uspto-grants-2013_08 |