Potassium tert-butoxide → HCID 58453204, compound

Participants

Reaction Steps

Potassium tert-butoxide (1.0 eq, 0.44 g, 3.62 mmol) was added slowly with stirring for 3 minutes to 32 ml of solution including methyltriphenylphosphonium bromide (1.2 eq, 1.55 g, 4.33 mmol) dissolved in THF. Then, the solution was stirred for 30 minutes at a room temperature and THF solution (35 ml) of trans-4-{4-[2-(4-propyl-cyclohexyl)ethenyl]phenyl}cyclohexane carbaldehyde (1.23 g, 3.62 mmol) obtained in Example 2-2 was added slowly dropwise for 10 minutes to reaction mixture, and then was stirred at a room temperature for 24 hours.

Provenance & Evidence