HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triacetoxyperiodinane → HCID 131730807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triacetoxyperiodinane | HCID 159087 | — |
| Reactant | HCID 131730808 | HCID 131730808 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131730807 | HCID 131730807 | 96% |
Reaction Steps
To a flask was added [6-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl]-methanol, methylene chloride, and Dess-Martin periodinane. The reaction was stirred, extracted, and the solvent was evaporated to provide the titled aldehyde in 96% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513214B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-b6cd13c1409c472eb94ada8079d75b17 |
| Source note | uspto-grants-2013_08 |