HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → Benzaldehyde, 4-(phenylmethoxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Benzaldehyde, 4-(phenylmethoxy)- | HCID 78109 | — |
Reaction Steps
4-hydroxy-benzaldehyde (57.64 g, 0.47 mol) and potassium carbonate (71.6 g, 0.51 mol), which were combined in acetone (200 mL), were reacted with benzyl bromine (80.73 g, 0.51 mol) and stirred at room temperature over night. The acetone was removed in vacuo, and the 4-Benzyloxy-benzaldehyde (71.6 g), as a white solid, is crystallized form ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513233B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-3400494bb96f44b3bb56b195696f21fd |
| Source note | uspto-grants-2013_08 |