HCID 54748151, compound → HCID 54748150, compound

Participants

Reaction Steps

N-((10S)-2-{[(4-fluoro-3-methylbenzyl)amino]carbonyl}-3-hydroxy-7,7-dimethyl-4-oxo-4,6,7,8,9,10-hexahydropyrimido[1,2-a]azepin-10-yl)-N,N′,N′-trimethylethanediamide. [α]D23° C.=−72.4° (c=0.5, MeOH); HRMS (ES+): 502.2481 (M+H); 1H NMR (400 MHz, CDCl3) δ 9.35 (br s, 3H), 7.2 (m, 2H), 6.9 (t, J=9 Hz, 1H), 5.34 (br s, 1H), 4.8 (d, J=14 Hz, 1H), 4.5 (m, 2H), 4.5 (m, 2H), 3.3 (d, J=14 Hz, 1H), 3.0 (s, 3H), 2.98, (s, 3H), 2.96 (s, 3H), 2.2 (s, 3H), 2.0 (m, 2H), 1.9 (m, 1H), 1.7 (s, 2H), 1.12 (s, 3H), 0.83 (s, 3H).

Provenance & Evidence