3-Bromotoluene → HCID 21350644, compound

HRID 1893289Notes

Reaction equation

Br[C:2]1[CH:3]=[C:4]([CH3:8])[CH:5]=[CH:6][CH:7]=1.[O:9]1[C:13]2([CH2:18][CH2:17][C:16](=[O:19])[CH2:15][CH2:14]2)[O:12][CH2:11][CH2:10]1>>[C:4]1([CH3:8])[CH:5]=[CH:6][CH:7]=[C:2]([C:16]2([OH:19])[CH2:17][CH2:18][C:13]3([O:12][CH2:11][CH2:10][O:9]3)[CH2:14][CH2:15]2)[CH:3]=1

Participants

Reactant 2

HCID 115603-Bromotoluene

HCID 5674151,4-Dioxaspiro[4.5]decan-8-one

Product 1

HCID 21350644HCID 21350644, compound

Procedure

The title compound was prepared as a white solid from 3-bromotoluene (Aldrich) and 1,4-dioxa-spiro[4.5]decan-8-one using the procedure described in Step A of Example 1.

Sources & evidence

ORD record: ord-4f2a2a50e6d2487a81d69cb8e014a8a6
Source dataset: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08513229B2

Reaction notes

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