HCID 86609227, compound → HCID 87543845, compound

HRID 1893398Notes

Reaction equation

HRID 1893398 reaction equation
[CH2:1]([O:8][N:9]=[C:10]([CH:17]([CH2:19][CH2:20][CH2:21][CH2:22]CC)C)[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:25].C(O[N:34]=[C:35](C(CCCCCC)C)[C:36]1C=CC=CC=1)C1C=CC=CC=1>>[ClH:25].[CH2:1]([O:8]/[N:9]=[C:10](\[CH:17]1[CH2:19][CH:20]2[CH2:21][CH2:22][N:34]1[CH2:35][CH2:36]2)/[C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 86609227HCID 86609227, compoundHCID 86609228HCID 86609228, compound

Product 1

HCID 87543845HCID 87543845, compound

Procedure

There are obtained 0.5 g of a fraction corresponding to (E)-1-azabicyclo[2.2.2.]oct-2-yl(phenyl)methanone O-benzyloxime and 2.25 g of another fraction corresponding to (Z)-1-azabicyclo[2.2.2.]oct-2-yl(phenyl)methanone O-benzyloxime hydrochloride

Workup

  1. customThere are obtained 0.5 g of a fraction corresponding to (E)-1-azabicyclo[2.2.2

Sources & evidence

ORD record
ord-a73440108a7a4425ac12a89fd3ddc60a
Source dataset
uspto-grants-2013_08
Patent number
US08513246B2

Reaction notes

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