2,6-Dimethylphenol → 2,6-Dimethylphenyl sulfamate

HRID 1893618Notes

Reaction equation

HRID 1893618 reaction equation
C1([O:4][S:5](=[O:8])(=[O:7])[NH2:6])CC1.[CH3:9][C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:11]=1[OH:17]>>[CH3:9][C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:11]=1[NH:6][S:5](=[O:7])(=[O:4])[O-:8].[CH3:9][C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:11]=1[O:17][S:5](=[O:7])(=[O:4])[NH2:6]

Participants

4

Reactant 2

HCID 113352,6-DimethylphenolHCID 57785190Cyclopropyl sulfamate

Product 2

HCID 124111032,6-Dimethylphenyl sulfamateHCID 866327872,6-Dimethylphenylsulfamate

Procedure

2,6-Dimethylphenylsulfamate was synthesized according to the method presented in the synthesis of sulfamic acid cyclopropyl ester in Example 1 with the exception of utilizing 2,6-dimethylphenol to obtain sulfamic acid 2,6-dimethyl-phenyl ester.

Sources & evidence

ORD record
ord-b5f5f83f316f43ba95dbb09b8154a81d
Source dataset
uspto-grants-2013_08
Patent number
US08513186B2

Reaction notes

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