Phenylsulfamate → 1-Methylcyclopropyl sulfamate

HRID 1893628Notes

Reaction equation

HRID 1893628 reaction equation
[C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH:6]=CC=[CH:3][CH:2]=1.CC1(O)CC1>>[CH3:6][C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 11030308PhenylsulfamateHCID 115644661-Methylcyclopropan-1-ol

Product 1

HCID 574867321-Methylcyclopropyl sulfamate

Procedure

Sulfamic acid 1-methyl-cyclopropyl ester was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing 1-methylcyclopropanol (synthesized by methods reported in Synthesis 1991, 234) to obtain sulfamic acid 1-methyl-cyclopropyl ester.

Workup

  1. customSulfamic acid 1-methyl-cyclopropyl ester was synthesized

Sources & evidence

ORD record
ord-b063ec42bde04c3fbb7d87c6c0bd57a1
Source dataset
uspto-grants-2013_08
Patent number
US08513186B2

Reaction notes

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