Phenylsulfamate → HCID 57785269, compound

HRID 1893638Notes

Reaction equation

[C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(C1(O)CC1)CC>>[CH2:6]([C:1]1([O:7][S:8](=[O:10])(=[O:11])[NH2:9])[CH2:2][CH2:3]1)[CH2:5][CH3:4]

Participants

Reactant 2

HCID 11030308Phenylsulfamate

HCID 130466221-Propylcyclopropanol

Product 1

HCID 57785269HCID 57785269, compound

Procedure

Sulfamic acid 1-propyl-cyclopropyl ester was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing 1-propylcyclopropanol (synthesized by methods reported in Synthesis 1991, 234) to obtain sulfamic acid 1-propyl-cyclopropyl ester.

Workup

customSulfamic acid 1-propyl-cyclopropyl ester was synthesized

Sources & evidence

ORD record: ord-638e3ea152af461d82da1d6f82c17d09
Source dataset: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08513186B2

Reaction notes

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