HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Phenylsulfonyl)aniline → (4-Benzenesulphonyl)phenyl-(6-iodo-7-fluoro-quinazolin-4-yl)-amine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Phenylsulfonyl)aniline | HCID 516666 | — |
| Reactant | 4-Chloro-7-fluoro-6-iodoquinazoline | HCID 21952006 | — |
| Product | (4-Benzenesulphonyl)phenyl-(6-iodo-7-fluoro-quinazolin-4-yl)-amine hydrochloride | HCID 68594451 | — |
Reaction Steps
Prepared according to Procedure A from 4-(benzenesulphonyl)phenylamine and 4-chloro-6-iodo-7-fluoroquinazoline. 1H NMR (400 MHz, DMSO-d6) δ: 10.89 (s, 1H), 9.3 (d, 1H), 8.79 (s, 1H), 8.07 (d, 2H), 8.0 (d, 2H), 7.94 (d, 2H), 7.67 (m, 2H), 7.61 (m, 2H). ESI-MS m/z 504 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513262B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-ec6e97fd4d084934a50cee780c8c4916 |
| Source note | uspto-grants-2013_08 |