HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1894184Generated: November 1, 2026
Dimethylformamide dimethyl acetal → (3E)-1-(3-bromophenyl)-3-(dimethylaminomethylidene)thiourea
https://huagongshe.com/reaction/1894184
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | (3-Bromophenyl)thiourea | HCID 2735619 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | (3E)-1-(3-bromophenyl)-3-(dimethylaminomethylidene)thiourea | HCID 58930371 | — |
Reaction Steps
(3-Bromophenyl)thiourea (2.1 g, 9.1 mmol) was suspended in N,N-dimethylformamide dimethyl acetal and was heated to 100° C. for 2 d. The cooled mixture was diluted with ether and filtered and the solid washed with ether to give the title compound (2.42 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08513276B2 |
|---|
| Source dataset | uspto-grants-2013_08 |
|---|
| ORD ID | ord-6a3488b0d32d424b9a0bff0e440f677e |
|---|
| Source note | uspto-grants-2013_08 |
|---|
