HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triphosgene → 6,6-Dimethyl-3-(6-(phenylethynyl)pyridazin-3-yl)-1,3-oxazinan-2-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triphosgene | HCID 94429 | — |
| Edukt | 2-Methyl-4-(6-phenylethynyl-pyridazin-3-ylamino)-butan-2-ol | HCID 57516775 | — |
| Produkt | 6,6-Dimethyl-3-(6-(phenylethynyl)pyridazin-3-yl)-1,3-oxazinan-2-one | HCID 53494699 | — |
Reaktionsschritte
The title compound, a crystalline light yellow solid, MS: m/e=308.3 (M+H+), was prepared in accordance with the general method of Example 152, step 2 starting from 2-methyl-4-(6-phenylethynyl-pyridazin-3-ylamino)-butan-2-ol (Example 153, step 1) and triphosgene.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08513273B2 |
| Quelldatensatz | uspto-grants-2013_08 |
| ORD ID | ord-0485dda2575f46b98666b7eba1f5b152 |
| Quellennotiz | uspto-grants-2013_08 |