HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11616635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11616091 | HCID 11616091 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 11616635 | HCID 11616635 | 75.2% |
Reaction Steps
2,3-dimethyl-4-(1,2,3,4-tetrahydroisoquinolin-2-yl)-1H-pyrrolo[3,2-c]pyridine (1.83 g, 6.59 mmol) prepared in Example 1 was dissolved in ethyl acetate (10 ml). The reaction mixture was saturated with hydrochloric acid gas and then filtered to give the titled compound as a white solid. (Yield: 75.2%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513277B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-3171073501524901b909fc7e56086684 |
| Source note | uspto-grants-2013_08 |