HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzyl bromide → HCID 66686584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzyl bromide | HCID 68021 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 11666896 | HCID 11666896 | — |
| Reactant | HCID 11666897 | HCID 11666897 | — |
| Product | HCID 66686584 | HCID 66686584 | 49.9% |
Reaction Steps
In accordance with the same procedures as in Example 47, except for using 1,2,3-trimethyl-4-(4-fluorobenzylamino)-1H-pyrrolo[3,2-c]pyridine obtained by treating the compound of Example 34 with a saturated sodium bicarbonate solution and 4-fluorobenzyl bromide, the titled compound was obtained as a white solid. (Yield: 49.9%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513277B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-bf863accc52b4b1bb941247ca408ad08 |
| Source note | uspto-grants-2013_08 |