HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Diazepan-5-one → HCID 25262577, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Diazepan-5-one | HCID 2737264 | — |
| Reactant | (4S,5R)-2-(6-tert-butyl-4-ethoxy-pyridin-3-yl)-4,5-bis-(4-chloro-phenyl)-4,5-dimethyl-4,5-dihydro-imidazole-1-carbonyl chloride | HCID 57669958 | — |
| Product | HCID 25262577 | HCID 25262577 | — |
Reaction Steps
In a manner analogous to the method described in examples 8, (4S,5R)-2-(6-tert-butyl-4-ethoxy-pyridin-3-yl)-4,5-bis-(4-chloro-phenyl)-4,5-dimethyl-4,5-dihydro-imidazole-1-carbonyl chloride (example 51) was coupled with [1,4]-diazepan-5-one (Oakwood) to give the title compound. HR-MS (ES, m/z) calculated for C34H40Cl2N5O3 [(M+H)+] 636.2503, observed 636.2504.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513239B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-eb2bd8d33be64a549ecbc4b0b2a1e902 |
| Source note | uspto-grants-2013_08 |