HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylamine → HCID 57669949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylamine | HCID 7912 | — |
| Reactant | {1-[(4S,5R)-2-(6-tert-butyl-4-ethoxy-pyridin-3-yl)-4,5-bis-(4-chloro-phenyl)-4,5-dimethyl-4,5-dihydro-imidazole-1-carbonyl]-piperidin-4-yl}-acetic acid | HCID 57670162 | — |
| Product | HCID 57669949 | HCID 57669949 | — |
Reaction Steps
In a manner analogous to the method described in example 163, {1-[(4S,5R)-2-(6-tert-butyl-4-ethoxy-pyridin-3-yl)-4,5-bis-(4-chloro-phenyl)-4,5-dimethyl-4,5-dihydro-imidazole-1-carbonyl]-piperidin-4-yl}-acetic acid was coupled with diisopropylamine (Aldrich) to give the title compound. HR-MS (ES, m/z) calculated for C42H55Cl2N5O3 [(M+H)+] 748.3755, observed 748.3758.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513239B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-82a658269fc5480995fb09c6ac08bea3 |
| Source note | uspto-grants-2013_08 |