Stannous Chloride → HCID 65440468, compound

Participants

Reaction Steps

To a 3 mL methanol solution of 2-(azidomethyl)-5-(1H-pyrazol-5-yl)-1,3,4-thiadiazole (50 mg, 0.24 mmol) was added Tin (II) chloride, anhydrous (82 mg. 0.43 mmol) and the resulting yellow solution was stirred at rt overnight. The reaction mixture was concentrated and purified by HPLC (acetonitrile-water-ammonium hydroxide eluent) to give the title compound (37 mg).

Provenance & Evidence