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HRID1895054

反应详情

EQUATION

反应方程式

HRID 1895054 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)OC(=O)N1CCC(CC2CCOCC2)(C(O)c2cc3cccc(F)c3s2)C1
HCID58017222

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCC(CC2CCOCC2)(C(=O)c2cc3cccc(F)c3s2)C1
HCID58017295

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[O]=[Mn]=[O]
催化剂HCID14801

Manganese oxide (Mn2O4)

MnO2

PROCEDURE

实验过程

3-(7-Fluoro-benzo[b]thiophene-2-carbonyl)-3-(tetrahydro-pyran-4-ylmethyl)-pyrrolidine-1-carboxylic acid tert-butyl ester was prepared from 3-[(7-fluoro-benzo[b]thiophen-2-yl)-hydroxy-methyl]-3-(tetrahydro-pyran-4-ylmethyl)-pyrrolidine-1-carboxylic acid tert-butyl ester by oxidation with MnO2 using the procedure of step 3 of Example 18.