HCID 49854235, compound → HCID 49854326, compound

Participants

Reaction Steps

To a solution of benzyl 2-(4-carbamoyl-1H-benzo[d]imidazol-2-yl)indoline-1-carboxylate (800 mg, 1.94 mmol) in ethyl acetate (50 ml) was added 10% Pd/C (80 mg) and the reaction mixture was degassed and stirred under H2 at 1 atmospheric pressure for 2 h at RT. The reaction mixture was filtered, the filtrate concentrated and the crude product was further triturated with ether to afford 2-(indolin-2-yl)-1H-benzo[d]imidazole-4-carboxamide. MS (ES+): m/z 279.1 [M+H]+

Provenance & Evidence