HRID1895955

反应详情

EQUATION

反应方程式

HRID 1895955 的结构方程式

PROCEDURE

实验过程

A well homogenised mixture of the Compound of Example 3 (20 mg, 0.93 mmol) and 2-fluoro-4-methoxynitrobenzene (21.3 mg, 0.12 mmol) was stirred at 120° C. for 0.5 h. The reaction crude was purified by flash chromatography (EtOAc—Petroleum Ether 1:1) affording the title product (21 mg).

WORKUP

后处理

  1. stirringwas stirred at 120° C. for 0.5 h
  2. customThe reaction crude
  3. customwas purified by flash chromatography (EtOAc—Petroleum Ether 1:1)