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HRID1895957

反应详情

EQUATION

反应方程式

HRID 1895957 的结构方程式

REACTANTS

反应物

3
结构：Ic1ccccc1
HCID11575

Benzene, iodo-

C6H5I

结构：CCOP(=O)(CC#C[Si](C)(C)C)OCC
HCID10933869

未命名化合物

结构：C#CC=C1CCN(c2ncccc2[N+](=O)[O-])CC1
HCID86627335

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cccnc1N1CCC(=CC#Cc2ccccc2)CC1
HCID25183673

未命名化合物

PROCEDURE

实验过程

The title compound was obtained as described for the Compound of Example 1, reacting Compound 1c with iodobenzene instead of 2-bromo-6-methylpyridine. Purification by flash chromatography with Petroleum Ether-EtOAc 65:35 afforded the title product.

WORKUP

后处理

  1. customPurification by flash chromatography with Petroleum Ether-EtOAc 65:35