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HRID1896000

反应详情

EQUATION

反应方程式

HRID 1896000 的结构方程式

REACTANTS

反应物

3
结构：Cc1ccc([N+](=O)[O-])c(Cl)n1
HCID1268230

2-chloro-6-methyl-3-nitropyridine

C6H5ClN2O2

结构：Cc1cccc(C#CC(O)C2CCNCC2)n1
HCID68977495

未命名化合物

结构：Fc1cc(F)cc(C#CCC2CCNCC2)c1
HCID68979491

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc([N+](=O)[O-])c(N2CCC(CC#Cc3cc(F)cc(F)c3)CC2)n1
HCID25181789

未命名化合物

PROCEDURE

实验过程

The title compound was prepared following the procedure described for the compound of Example 237, but using Compound 248a instead of Compound 237a and 2-chloro-3-nitro-6-picoline instead of 2-bromo-3-nitropyridine. The crude was purified by automated flash liquid chromatography (Horizon™-Biotage) eluting with Petroleum Ether-EtOAc 9:1, affording the title product as a yellow oil.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customThe crude was purified by automated flash liquid chromatography (Horizon™-Biotage)
  3. washeluting with Petroleum Ether-EtOAc 9:1